ASTM D322 for gasoline diluent in used gasoline engine oils by distillation
4. Summary of Test Method
4.1 The sample, mixed with water, is placed in a glass still provided with a reflux condenser discharging into a graduated trap connected to the still. Heat is applied, and the contents of the still are brought to boiling. The diluent in the sample is vaporized with the water and then liquefied in the condenser. The diluent collects at the top of the trap, and the excess water runs back to the still where it is again vaporized, carrying over an additional quantity of diluent. The boiling is continued until all the diluent has been boiled out and recovered in the trap. The volume is recorded.

5. Significance and Use
5.1 Some fuel dilution of the engine oil may take place during normal operation. However, excessive fuel dilution is of concern in terms of possible performance problems.